Reaktionsgleichung
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[N:9]1[CH2:14][CH2:13][N:12]([CH2:15][CH2:16][CH2:17][CH2:18]O)[CH2:11][CH2:10]1.[CH2:20]([NH:23][CH:24]1[CH2:32][CH2:31][C:27]2[N:28]=[CH:29][S:30][C:26]=2[CH2:25]1)[CH2:21]C>>[CH2:20]([N:23]([CH2:18][CH2:17][CH2:16][CH2:15][N:12]1[CH2:13][CH2:14][N:9]([C:4]2[CH:5]=[CH:6][CH:7]=[CH:8][C:3]=2[O:2][CH3:1])[CH2:10][CH2:11]1)[CH:24]1[CH2:32][CH2:31][C:27]2[N:28]=[CH:29][S:30][C:26]=2[CH2:25]1)[CH3:21]Komponenten
3
Versuchsvorschrift
Compound 30 is prepared from 30A and 1C as described for 1. The salt of oxalic acid is crystallized from ethanol/diethylether.
Aufarbeitung
- customThe salt of oxalic acid is crystallized from ethanol/diethylether
Quellen und Nachweise
- ORD-Eintrag
- ord-570c7c7c30274ae09247e0ce6ae586ee
- Quelldatensatz
- uspto-grants-2013_03
- Patentnummer
- US08389555B2
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