5-Amino-2-(trifluoromethyl)pyridine → 6-(Trifluoromethyl)pyridine-3-sulfonyl chloride
Reaktionsgleichung
Cl[C:2]1[CH:3]=[C:4]([S:12]([Cl:15])(=[O:14])=[O:13])[CH:5]=C[C:7]=1[C:8]([F:11])([F:10])[F:9].FC(F)(F)C1[N:23]=CC(N)=CC=1>>[F:9][C:8]([F:11])([F:10])[C:7]1[N:23]=[CH:5][C:4]([S:12]([Cl:15])(=[O:14])=[O:13])=[CH:3][CH:2]=1Komponenten
3
Versuchsvorschrift
The title compound was prepared by a method analogous to the method used to prepare Intermediate 39 using 6-(trifluoromethyl)pyridin-3-amine as the starting material. LCMS (R—SO3−)=226.2.
Quellen und Nachweise
- ORD-Eintrag
- ord-b783f24728a646a48c1bbd35ad8de7fb
- Quelldatensatz
- uspto-grants-2013_03
- Patentnummer
- US08394858B2
Notizen zur Reaktion
Wird geladen…