Methylamine → HCID 67153355, Verbindung
Reaktionsgleichung
CS(OCCCOC1C=CC=C(C2N(C3C=CC=C(Cl)C=3)N=C(C(N3CC(=O)NC3)=O)C=2)C=1)(=O)=O.CN.[CH:38]([OH:40])=[O:39].[Cl:41][C:42]1[CH:43]=[C:44]([N:48]2[C:52]([C:53]3[CH:58]=[CH:57][CH:56]=[C:55]([O:59][CH2:60][CH2:61][CH2:62][N:63](C)[CH3:64])[CH:54]=3)=[CH:51][C:50]([C:66]([N:68]3[CH2:72][C:71](=[O:73])[NH:70][CH2:69]3)=[O:67])=[N:49]2)[CH:45]=[CH:46][CH:47]=1>O1CCCC1>[CH:38]([OH:40])=[O:39].[Cl:41][C:42]1[CH:43]=[C:44]([N:48]2[C:52]([C:53]3[CH:58]=[CH:57][CH:56]=[C:55]([O:59][CH2:60][CH2:61][CH2:62][NH:63][CH3:64])[CH:54]=3)=[CH:51][C:50]([C:66]([N:68]3[CH2:72][C:71](=[O:73])[NH:70][CH2:69]3)=[O:67])=[N:49]2)[CH:45]=[CH:46][CH:47]=1Komponenten
5
Edukt 3
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
The preparation of the title compound takes place starting from the compound of Example 120A and methylamine without the addition of tetrahydrofuran in analogy to the synthesis of the compound of Example 29. 46 mg (44% of theory) of the title compound are obtained.