(E)-2-(4,6-difluoro-1-indanylidene)acetic acid → (E)-2-(4-fluoro-1-indanylidene)acetyl Chloride

HRID 1954877Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1954877
[F:1][C:2]1[CH:10]=[C:9](F)[CH:8]=[C:7]2[C:3]=1[CH2:4][CH2:5]/[C:6]/2=[CH:12]\[C:13]([Cl:15])=[O:14].FC1C=C(F)C=C2C=1CC/C/2=C\C(O)=O>>[F:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]2[C:3]=1[CH2:4][CH2:5]/[C:6]/2=[CH:12]\[C:13]([Cl:15])=[O:14]

Komponenten

3

Edukt 2

HCID 10976722(E)-2-(4,6-difluoro-1-indanylidene)acetic acidHCID 10977254(E)-2-(4,6-difluoro-1-indanylidene)acetyl Chloride

Produkt 1

HCID 23293683(E)-2-(4-fluoro-1-indanylidene)acetyl Chloride

Versuchsvorschrift

This compound was prepared in a similar manner to (E)-2-(4,6-difluoro-1-indanylidene)acetyl chloride in Example 5f by substituting (E)-2-(4-fluoro-1-indanylidene)acetic acid (5.77 g, 0.03 mol) for (E)-2-(4,6-difluoro-1-indanylidene)acetic acid. The resulting solution was concentrated in vacuo, and the residue was used without further purification.

Aufarbeitung

  1. concentrationThe resulting solution was concentrated in vacuo
  2. customthe residue was used without further purification

Quellen und Nachweise

ORD-Eintrag
ord-59fa4e41488045dbb7d7eb0f6afca2ba
Quelldatensatz
uspto-grants-2000_09
Patentnummer
US06124284

Notizen zur Reaktion

Wird geladen…