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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1955461Erstellt: 25. Oktober 2026

Hydrogen Bromide → 6-Hydroxy-1,2,3,4-tetrahydronaphthalene-2-carboxylic acid

https://huagongshe.com/reaction/1955461

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktHydrogen BromideHCID 260—
Edukt2-Naphthalenecarboxylic acid, 6-(decyloxy)-HCID 10359167—
LösungsmittelAcetic AcidHCID 176—
Produkt6-Hydroxy-1,2,3,4-tetrahydronaphthalene-2-carboxylic acidHCID 19070001100%

Reaktionsschritte

16.6 g (50 mmol) of the 6-decyloxynaphthalene-2-carboxylic acid obtained in the first stage was heated under reflux at 130° C. for 7 hours in the presence of 250 cc of acetic acid and 86.5 g (0.5 mol) of 47% hydrobromic acid. To the reaction mixture was added distilled water, and then the resulting mixture was concentrated under reduced pressure to obtain 10.60 g (50 mmol) of 1,2,3,4-tetrahydro-6-hydroxynaphthalene-2-carboxylic acid.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05776365
Quelldatensatzuspto-grants-1998_07
ORD IDord-bce8560a0c644c2bb4ff2578e5abcfbc
Quellennotizuspto-grants-1998_07