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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1959998Erstellt: 26. Oktober 2026

Methyl iodide → HCID 178480658, Verbindung

https://huagongshe.com/reaction/1959998

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktMethyl iodideHCID 6328—
Edukt1-(4-Chlorophenyl)-1H-imidazoleHCID 142859—
LösungsmittelTetrahydrofuranHCID 8028—
ProduktHCID 178480658HCID 178480658—

Reaktionsschritte

1-(4-Chlorophenyl)imidazole (0.37 g, 2.07 mmol) is dissolved in THF (5 ml) and subsequently admixed with methyl iodide (1.47 g, 10.4 mmol) and allowed to stand for 20 hours. The precipitate formed is subsequently filtered off and washed with ethanol and with petroleum ether and subsequently dried under reduced pressure. This gives 0.46 g of 1-(4-chlorophenyl)-3-methylimidazolium iodide.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08410280B2
Quelldatensatzuspto-grants-2013_04
ORD IDord-5ba2519728b1474aaa39a8a35afc3e46
Quellennotizuspto-grants-2013_04