Allylamine → HCID 21490733, Verbindung
Reaktionsgleichung
[C:1]([OH:13])(=O)[CH2:2][CH:3]1[CH:11]=[CH:10][CH2:9][CH2:8][CH:4]1[C:5]([OH:7])=O.[CH2:14]([NH2:17])[CH:15]=[CH2:16]>>[CH2:14]([N:17]1[C:1](=[O:13])[CH2:2][C:3]2[CH2:11][CH2:10][CH2:9][CH2:8][C:4]=2[C:5]1=[O:7])[CH:15]=[CH2:16]Komponenten
3
Versuchsvorschrift
A mixture of tetrahydrohomophthalic acid (9.2 g., 0.05 mole) and allylamine (2.8 g., 0.05 mole) is heated by an oil bath until molten for 40 minutes. The mixture solidifies upon cooling, and is recrystallized twice from isopropanol, giving 2-allyl-5,6,7,8-tetrahydroisoquinoline-1,3(2H, 4H)-dione.
Aufarbeitung
- temperatureis heated by an oil bath until molten for 40 minutes
- temperatureupon cooling
- customis recrystallized twice from isopropanol
Quellen und Nachweise
- ORD-Eintrag
- ord-dc18d779806e4351ac8fc00a11e9100e
- Quelldatensatz
- uspto-grants-1976_12
- Patentnummer
- US03998954
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