HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cyclopentyl isothiocyanate → N-[5-Chloro-3-(cyclopentylthiocarbamoyl)sulfamoylthiophen-2-yl]acetamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cyclopentyl isothiocyanate | HCID 141792 | — |
| Edukt | N-(5-chloro-3-sulfamoylthiophen-2-yl)-acetamide | HCID 22000000 | — |
| Produkt | N-[5-Chloro-3-(cyclopentylthiocarbamoyl)sulfamoylthiophen-2-yl]acetamide | HCID 21999997 | — |
Reaktionsschritte
The title compound was prepared from N-(5-chloro-3-sulfamoylthiophen-2-yl)-acetamide and cyclopentyl isothiocyanate by a procedure analogous to the procedure described in example 15a (yield of crude product: 93%); 1H-NMR (DMSO-d6): δ1.3-2.0 (m, 8H, (CH2)4), 2.28 (s, 3H, CH3), 4.32 (sext, 1H, CH), 7.16 (s, 1H, H-4), 8.48 (br d, 1H, NH), 10.23 (br s, 1H, NH).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06225310B1 |
| Quelldatensatz | uspto-grants-2001_05 |
| ORD ID | ord-54ab9b7d65824b2a83913917efb5b319 |
| Quellennotiz | uspto-grants-2001_05 |