Tetrahydrofuran → Ethyl Tetrahydrofuran-2-acetate

HRID 1976571Notizen

Reaktionsgleichung

[CH3:1][CH2:2][O:3]/[C:4](/[O-:8])=[CH:5]/[N+]#N.[O:9]1[CH2:13][CH2:12][CH2:11][CH2:10]1>>[O:9]1[CH2:13][CH2:12][CH2:11][CH:10]1[CH2:5][C:4]([O:3][CH2:2][CH3:1])=[O:8]

Komponenten

Edukt 2

HCID 8028Tetrahydrofuran

HCID 178472844HCID 178472844, Verbindung

Produkt 1

HCID 551345Ethyl Tetrahydrofuran-2-acetate

Versuchsvorschrift

Following the procedure of Preparative Example 14, 2.0 g (17.5 mmol) of ethyl diazo acetate was reacted with tetrahydrofuran to give 1.7 g of the product as a colorless oil, bp 84°-86° C. at 20 mm Hg.

Quellen und Nachweise

ORD-Eintrag: ord-6d7bfc7a73ab4d2cac900313277c21ea
Quelldatensatz: uspto-grants-2001_05
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06228865B1

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