HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetanilide → N-(6-methyl-2-pyridyl)acetanilide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetanilide | HCID 904 | — |
| Edukt | 6-Chloro-2-picoline | HCID 87601 | — |
| Produkt | N-(6-methyl-2-pyridyl)acetanilide | HCID 21993566 | 7% |
Reaktionsschritte
Using acetanilide (9.16 g) and 2-chloro-6-methylpyridine (17.3 g), a reaction was made in the same manner as in 1) of Production Example 14. The subsequent purification by silica gel chromatography (developing solvent, ethyl acetate:hexane=1:1, ethyl acetate) produced N-(6-methyl-2-pyridyl)acetanilide (1.07 g; yield, 7%) as a pale brown oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06235730B1 |
| Quelldatensatz | uspto-grants-2001_05 |
| ORD ID | ord-4bf9e1b3d0e24bc0b7a5e25de7e74f10 |
| Quellennotiz | uspto-grants-2001_05 |