1-Carboxy-3,5,7-trihydroxyadamantane → 1-Carboxy-3,5-dihydroxy-7-acryloyloxyadamantane

HRID 1978119

Reaktionsgleichung

Reaktionsgleichung von HRID 1978119
[C:1](OCC12CC3CC(CC(O)(C3)C1)C2)(=[O:4])[CH:2]=[CH2:3].[C:18]([C:21]12[CH2:31][C:25]3([OH:32])[CH2:26][C:27]([OH:30])([CH2:29][C:23]([OH:33])([CH2:24]3)[CH2:22]1)[CH2:28]2)([OH:20])=[O:19]>>[C:18]([C:21]12[CH2:22][C:23]3([OH:33])[CH2:24][C:25]([O:32][C:1](=[O:4])[CH:2]=[CH2:3])([CH2:26][C:27]([OH:30])([CH2:29]3)[CH2:28]1)[CH2:31]2)([OH:20])=[O:19]

Komponenten

3

Edukt 2

HCID 120393761-Carboxy-3,5,7-trihydroxyadamantaneHCID 219967831-Hydroxy-3-(acryloyloxymethyl)adamantane

Produkt 1

HCID 219968051-Carboxy-3,5-dihydroxy-7-acryloyloxyadamantaneAusbeute 81 %

Versuchsvorschrift

The reaction was conducted in the same manner as said (2) except that 1-carboxy-3,5,7-trihydroxyadamantane was used instead of the 1-carboxy-3,5-dihydroxyadamantane, and, as a result, a 1-carboxy-3,5-dihydroxy-7-acryloyloxyadamantane (yield: 81%, white solid) was produced.

Quellen und Nachweise

ORD-Eintrag
ord-15c0f8870d354862a32b5f49c9a3e085
Quelldatensatz
uspto-grants-2001_05
Patentnummer
US06235851B1

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