HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ammonia → 3-Methoxy-5-methylpyrazine-2-carboxamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ammonia | HCID 222 | — |
| Edukt | Methyl 3-methoxy-5-methylpyrazine-2-carboxylate | HCID 21702987 | — |
| Produkt | 3-Methoxy-5-methylpyrazine-2-carboxamide | HCID 11062776 | 87% |
Reaktionsschritte
1 g (5.5 mmol) of methyl 3-methoxy-5-methylpyrazine-carboxylate was initially charged in 15 ml (198 mmol) of NH3 (25%) and the mixture was stied at 50° C. After concentration, 0.8 g of 3-methoxy-5-methylpyrazine-2carboxamide was obtained. The yield was 86 percent. Other data concerning the title product was:
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06235905B1 |
| Quelldatensatz | uspto-grants-2001_05 |
| ORD ID | ord-5ae1cef7b8154ee1815fb4d0c6ec7b33 |
| Quellennotiz | uspto-grants-2001_05 |