Hydrochloric Acid → HCID 70247330, Verbindung

HRID 1978418Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1978418
C(OC([N:8]1[CH2:13][CH2:12][CH:11]([CH2:14][NH:15][C:16](=[O:31])[CH:17]=[CH:18][C:19]2[S:29][C:28]3[N:30]4[C:21](=[CH:22][N:23]=[C:24]4[CH:25]=[CH:26][CH:27]=3)[CH:20]=2)[CH2:10][CH2:9]1)=O)(C)(C)C.[ClH:32]>C(O)C>[ClH:32].[ClH:32].[NH:8]1[CH2:13][CH2:12][CH:11]([CH2:14][NH:15][C:16](=[O:31])[CH:17]=[CH:18][C:19]2[S:29][C:28]3[N:30]4[C:21](=[CH:22][N:23]=[C:24]4[CH:25]=[CH:26][CH:27]=3)[CH:20]=2)[CH2:10][CH2:9]1

Komponenten

4

Edukt 2

HCID 313Hydrochloric AcidHCID 70248359HCID 70248359, Verbindung

Produkt 1

HCID 70247330HCID 70247330, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

To this crude N-[1-(tert-butoxycarbonyl)piperidin-4-ylmethyl]-3-(5-thia-1,8b-diazaacenaphthylen-4-yl)acrylamide was added 1 ml of concentrated hydrochloric acid and the mixture was stirred at room temperature for 0.5 hour. After addition of ethanol, the mixture was stirred and the resulting precipitate was collected and washed serially with ethanol and diethyl ether to provide the title compound.

Aufarbeitung

  1. stirringthe mixture was stirred
  2. customthe resulting precipitate was collected
  3. washwashed serially with ethanol and diethyl ether

Quellen und Nachweise

ORD-Eintrag
ord-373810fc5d264c3893955c649536d98b
Quelldatensatz
uspto-grants-2001_05
Patentnummer
US06235731B1

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