Dimethylformamide → N,N,N,2,2-Pentamethylpropan-1-aminium iodide

Reaktionsgleichung

[CH2:1](N)[C:2](C)([CH3:4])[CH3:3].[CH2:7](N(CCCC)CCCC)CCC.C[I:21].[CH3:22][N:23]([CH:25]=O)[CH3:24]>>[I-:21].[CH3:22][N+:23]([CH2:25][C:2]([CH3:4])([CH3:3])[CH3:1])([CH3:7])[CH3:24]

Komponenten

Edukt 4

HCID 6228Dimethylformamide

HCID 6328Methyl iodide

HCID 7622Tributylamine

HCID 79882Neopentylamine

Produkt 1

HCID 13652289N,N,N,2,2-Pentamethylpropan-1-aminium iodide

Versuchsvorschrift

11.51 Grams of neopentylamine (Aldrich), 48.7 grams of tributyl amine and 100 ml of DMF were mixed and cooled. 56 Grams of methyl iodide (Aldrich) were added dropwise and the reaction as carried out and worked up as in Example 1.

Aufarbeitung

temperaturecooled
customthe reaction

Quellen und Nachweise

ORD-Eintrag: ord-b24055098b804e3ea5487e19d09e7b90
Quelldatensatz: uspto-grants-1985_04
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US04510256

Notizen zur Reaktion

Wird geladen…