Methyl[(morpholin-4-yl)sulfanyl]carbamyl fluoride → HCID 86739197, Verbindung
Reaktionsgleichung
[N:1](=[C:3]1[C:8]([CH:9]([CH3:11])[CH3:10])=[N:7][CH2:6][CH2:5][S:4]1)[OH:2].[CH3:12][N:13]([S:17][N:18]1[CH2:23][CH2:22][O:21][CH2:20][CH2:19]1)[C:14](F)=[O:15]>>[CH3:12][N:13]([S:17][N:18]1[CH2:19][CH2:20][O:21][CH2:22][CH2:23]1)[C:14]([O:2][N:1]=[C:3]1[C:8]([CH:9]([CH3:11])[CH3:10])=[N:7][CH2:6][CH2:5][S:4]1)=[O:15]Komponenten
3
Versuchsvorschrift
2-Oxo-5,6-dihydro-3-isopropyl-2H-1,4-thiazine oxime is reacted with N-methyl-N-morpholinosulphenylcarbamoyl fluoride as described in Example 25 to yield 2-oxo-5,6-dihydro-3-isopropyl-2H-1,4-thiazine O-(N-methyl-N-morpholinosulphenylcarbamoyl)oxime, m.p. 127°-128.5° C.
Quellen und Nachweise
- ORD-Eintrag
- ord-47848c593e164f8f9aee8edb6d7f0ed3
- Quelldatensatz
- uspto-grants-1985_04
- Patentnummer