HCID 57719660, Verbindung → HCID 57719575, Verbindung
Reaktionsgleichung
C(OC([NH:8][C:9]1[N:14]=[CH:13][C:12]([CH2:15][O:16][C:17]([NH:19][CH2:20][C:21]2[CH:22]=[C:23]([CH2:27][C@H:28]([O:32][CH:33]([CH3:35])[CH3:34])[C:29]([OH:31])=[O:30])[CH:24]=[CH:25][CH:26]=2)=[O:18])=[CH:11][CH:10]=1)=O)(C)(C)C>FC(F)(F)C(O)=O>[NH2:8][C:9]1[N:14]=[CH:13][C:12]([CH2:15][O:16][C:17]([NH:19][CH2:20][C:21]2[CH:22]=[C:23]([CH2:27][C@H:28]([O:32][CH:33]([CH3:35])[CH3:34])[C:29]([OH:31])=[O:30])[CH:24]=[CH:25][CH:26]=2)=[O:18])=[CH:11][CH:10]=1Komponenten
3
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
3-{3-[(6-t-Butoxycarbonylaminopyridin-3-ylmethoxycarbonylamino)methyl]phenyl}-2(S)-isopropoxypropanoic acid was dissolved in trifluoroacetic acid, and the mixture was concentrated. The residue was purified by reverse-phase high performance liquid chromatography, to give the title compound.
Aufarbeitung
- concentrationthe mixture was concentrated
- customThe residue was purified by reverse-phase high performance liquid chromatography