tert-butyl (1S,2S)-1-benzyl-2-hydroxyhexylcarbamate → HCID 69077819, Verbindung
Reaktionsgleichung
[F:1][C:2]1[CH:3]=[C:4]([CH:21]=[C:22]([F:24])[CH:23]=1)[CH2:5][C@@H:6]([NH:13]C(=O)OC(C)(C)C)[C@@H:7]([OH:12])[CH2:8][CH2:9][CH2:10][CH3:11].C([C@H](NC(=O)OC(C)(C)C)[C@@H](O)CCCC)C1C=CC=CC=1>>[NH2:13][C@@H:6]([C@@H:7]([OH:12])[CH2:8][CH2:9][CH2:10][CH3:11])[CH2:5][C:4]1[CH:21]=[C:22]([F:24])[CH:23]=[C:2]([F:1])[CH:3]=1Komponenten
3
Versuchsvorschrift
Prepared from the Boc removal of the anti diastereoisomer tert-butyl (1R,2S)-1-(3,5-difluorobenzyl)-2-hydroxyhexylcarbamate using a similar procedure as described in intermediate I step D. ES MS (M+H)=244.
Quellen und Nachweise
- ORD-Eintrag
- ord-967c2d9164e841b3af5943ad36a7ca7f
- Quelldatensatz
- uspto-grants-2009_06
- Patentnummer
- US07550481B2
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