1-(Bromomethyl)-3-chlorobenzene → HCID 68705060, Verbindung
Reaktionsgleichung
[CH2:1]([O:3][C:4]1[CH:22]=[CH:21][CH:20]=[CH:19][C:5]=1[CH2:6][O:7][C:8]1[CH:13]=[CH:12][N:11]=[C:10]2[C:14]([CH3:18])=[C:15]([CH3:17])[NH:16][C:9]=12)[CH3:2].[Cl:23][C:24]1[CH:25]=[C:26]([CH:29]=[CH:30][CH:31]=1)[CH2:27]Br>>[ClH:23].[Cl:23][C:24]1[CH:25]=[C:26]([CH:29]=[CH:30][CH:31]=1)[CH2:27][N:16]1[C:9]2[C:10](=[N:11][CH:12]=[CH:13][C:8]=2[O:7][CH2:6][C:5]2[CH:19]=[CH:20][CH:21]=[CH:22][C:4]=2[O:3][CH2:1][CH3:2])[C:14]([CH3:18])=[C:15]1[CH3:17]Komponenten
3
Versuchsvorschrift
In accordance with the same procedures as in Step 2 of Example 33, except for using 7-(2-ethoxybenzyloxy)-2,3-dimethyl-1H-pyrrolo[3,2-b]pyridine prepared in Step 2 and 3-chlorobenzyl bromide, the titled compound was obtained as a white solid. (Yield: 79.8%)
Quellen und Nachweise
- ORD-Eintrag
- ord-1a9eca2fb9314c67a3884fcf41f0d1bb
- Quelldatensatz
- uspto-grants-2010_01