Methanol → Methyl 4-(methylamino)butanoate

HRID 1991590Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1991590
Cl.[CH3:2][NH:3][CH2:4][CH2:5][CH2:6][C:7]([OH:9])=[O:8].S(Cl)(Cl)=O.[CH3:14]O>>[CH3:14][O:8][C:7](=[O:9])[CH2:6][CH2:5][CH2:4][NH:3][CH3:2]

Komponenten

4

Edukt 3

HCID 887MethanolHCID 24386Thionyl ChlorideHCID 126266544-(Methylamino)butyric acid hydrochloride

Produkt 1

HCID 14769104Methyl 4-(methylamino)butanoate

Reaktionsbedingungen

Temperatur
0 °C

Versuchsvorschrift

4-(methylamino) butyric acid HCl was dissolved in methanol and thionyl chloride in catalytic amount was added drop by drop. The reaction mixture was stirred at 0° C. for 30 min. Thereafter, the solvent was reduced in vacu, yielding a white solid.

Aufarbeitung

  1. customyielding a white solid

Quellen und Nachweise

ORD-Eintrag
ord-a3dd38a54c534097bca325db7a81d19e
Quelldatensatz
uspto-grants-2010_01
Patentnummer
US07645903B2

Notizen zur Reaktion

Wird geladen…