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HRID 1995483Erstellt: 25. Oktober 2026

Pyridine → N-(chloroacetoxy)-3-chloro-N-(2-chlorophenyl)methyl-2,2-dimethylpropanamide

https://huagongshe.com/reaction/1995483

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPyridineHCID 1049—
EduktChloroacetyl chlorideHCID 6577—
Edukt3-chloro-N-(2-chlorophenyl)methyl-N-hydroxy-2,2-dimethylpropanamideHCID 9925558—
LösungsmittelTolueneHCID 1140—
ProduktN-(chloroacetoxy)-3-chloro-N-(2-chlorophenyl)methyl-2,2-dimethylpropanamideHCID 13192525—

Reaktionsschritte

This compound was prepared in the manner of Example 13, using 4.0 g (0.014 mole) of 3-chloro-N-(2-chlorophenyl)methyl-N-hydroxy-2,2-dimethylpropanamide (prepared in Example 1), 1.6 g (0.014 mole) of chloroacetyl chloride, and 1.2 g (0.015 mole) of pyridine, in 50 ml toluene. The product was a liquid, of which nmr and ir spectra were consistent with the assigned structure.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04405357
Quelldatensatzuspto-grants-1983_09
ORD IDord-9ad350d0eae44ae09e8fa8044bb1c917
Quellennotizuspto-grants-1983_09