HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
7-Benzyl-1-ethoxymethyl-3-methylxanthine → HCID 9815938, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 7-Benzyl-1-ethoxymethyl-3-methylxanthine | HCID 19689145 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | HCID 9815938 | HCID 9815938 | — |
Reaktionsschritte
17.5 g (0.056 mol) of 7-benzyl-1-ethoxymethyl-3-methylxanthine were hydrogenated over 1.8 g of palladium (10%) on activated carbon at room temperature for 8 hours in 500 ml of ethanol. The catalyst was filtered off and the filtrate was concentrated to dryness and crystallized from dimethylformamide/diisopropyl ether.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05728686 |
| Quelldatensatz | uspto-grants-1998_03 |
| ORD ID | ord-8274ed2fb34e4d4d9f44b77cbe179a49 |
| Quellennotiz | uspto-grants-1998_03 |