Triethylsilicon → tert-butyl 6-formyl-8-phenylmethoxy-3,4-dihydro-1H-isoquinoline-2-carboxylate

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	Triethylsilicon	HCID 6327258	—
Edukt	1-Methyl-1,1-diphenylsilanecarboxylic acid	HCID 67974019	—
Edukt	tert-butyl 6-bromo-8-phenylmethoxy-3,4-dihydro-1H-isoquinoline-2-carboxylate	HCID 132189892	—
Reagenz	Diisopropylethylamine	HCID 81531	—
Reagenz	(3R,4R,5R,6R)-5-acetamido-2-[[(2R,3S,4R,5R)-5-(4-amino-2-oxopyrimidin-1-yl)-3,4-dihydroxyoxolan-2-yl]methoxy-hydroxyphosphoryl]oxy-3-fluoro-4-hydroxy-6-[(1R,2R)-1,2,3-trihydroxypropyl]oxane-2-carboxylic acid	HCID 448383	—
Katalysator	palladium(II) acetate	HCID 167845	—
Katalysator	HCID 178420544	HCID 178420544	—
Lösungsmittel	Dimethylformamide	HCID 6228	—
Produkt	tert-butyl 6-formyl-8-phenylmethoxy-3,4-dihydro-1H-isoquinoline-2-carboxylate	HCID 132190424	—
Interner Standard	9-Phenylanthracene	HCID 11766	—

Temperatur	90 °C