HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Carbonate → Diethyl 5-hydroxypentylphosphonate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Carbonate | HCID 10340 | — |
| Edukt | 5-(Diethylphosphono)pentyl acetate | HCID 19689222 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | Diethyl 5-hydroxypentylphosphonate | HCID 10680635 | — |
Reaktionsschritte
92 g (0.345 mol) of 5-(diethylphosphono)pentyl acetate were heated at 50° C. for 10 hours with stirring with 74 g (0.7 mol) of finely powdered sodium carbonate in 500 ml of methanol. The solution was filtered, concentrated and distilled in a bulb tube.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05728686 |
| Quelldatensatz | uspto-grants-1998_03 |
| ORD ID | ord-c88ff47b784b42e596807b91fc6e4cda |
| Quellennotiz | uspto-grants-1998_03 |