N-BOC-ethylenediamine → HCID 178489244, Verbindung
Reaktionsgleichung
[CH3:1][O:2][C:3]1[CH:21]=[C:20]([CH:22]=[C:23]2[S:27][C:26](SC)=[N:25][C:24]2=[O:30])[CH:19]=[CH:18][C:4]=1[O:5][C:6]1[CH:13]=[CH:12][C:9]([C:10]#[N:11])=[CH:8][C:7]=1[C:14]([F:17])([F:16])[F:15].[C:31]([O:35][C:36](=[O:41])[NH:37][CH2:38][CH2:39][NH2:40])([CH3:34])([CH3:33])[CH3:32]>>[C:31]([O:35][C:36](=[O:41])[NH:37][CH2:38][CH2:39][NH:40][C:26]1[S:27][C:23](=[CH:22][C:20]2[CH:19]=[CH:18][C:4]([O:5][C:6]3[CH:13]=[CH:12][C:9]([C:10]#[N:11])=[CH:8][C:7]=3[C:14]([F:15])([F:17])[F:16])=[C:3]([O:2][CH3:1])[CH:21]=2)[C:24](=[O:30])[N:25]=1)([CH3:34])([CH3:32])[CH3:33]Komponenten
3
Versuchsvorschrift
(2-{5-[4-(4-Cyano-2-trifluoromethyl-phenoxy)-3-methoxy-benzylidene]-4-oxo-4,5-dihydro-thiazol-2-ylamino}-ethyl)-carbamic acid tert-butyl ester was prepared using 4-[2-Methoxy-4-(2-methylsulfanyl-4-oxo-4H-thiazol-5-ylidenemethyl)-phenoxy]-3-trifluoromethyl-benzonitrile and (2-Amino-ethyl)-carbamic acid tert-butyl ester as described in Example 5C.
Quellen und Nachweise
- ORD-Eintrag
- ord-961c529dbfe84ef8a2c3195b905895cf
- Quelldatensatz
- uspto-grants-2013_11