3-(3-Chlorophenyl)-2-propynal → 3-(3-Chlorophenyl)prop-2-ynal oxime

HRID 2040862Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2040862
[C:1]1([C:7]#[C:8][CH:9]=[N:10][OH:11])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Cl:12]C1C=C(C#CC=O)C=CC=1>>[Cl:12][C:3]1[CH:2]=[C:1]([C:7]#[C:8][CH:9]=[N:10][OH:11])[CH:6]=[CH:5][CH:4]=1

Komponenten

3

Edukt 2

HCID 468725403-(3-Chlorophenyl)-2-propynalHCID 765430553-Phenylprop-2-ynal oxime

Produkt 1

HCID 765430563-(3-Chlorophenyl)prop-2-ynal oximeAusbeute 96,4 %

Versuchsvorschrift

The title compound was prepared following the method here described for Compound 1a, using Compound 31d instead of phenylpropiolaldehyde. The pale brown residue was used in the next step without further purification. Yield: 96.4%.

Aufarbeitung

  1. customThe pale brown residue was used in the next step without further purification

Quellen und Nachweise

ORD-Eintrag
ord-a3b51d3f27f14f879e822be58fb81423
Quelldatensatz
uspto-grants-2013_11
Patentnummer
US08580962B2

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