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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2042388Erstellt: 27. Oktober 2026

Piperonal → Bis(3,4-methylenedioxy)chalcone

https://huagongshe.com/reaction/2042388

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPiperonalHCID 8438—
EduktSodium HydroxideHCID 14798—
EduktAcetopiperoneHCID 76622—
LösungsmittelEthanolHCID 702—
ProduktBis(3,4-methylenedioxy)chalconeHCID 294346—

Reaktionsschritte

A mixture of piperonal (460 mg) and 3,4-methylenedioxyacetophenone (500 mg) in ethanol (20 ml) was treated with 1M NaOH solution (4 ml), then the mixture was stirred overnight. The pale yellow crystalline solid was filtered off, washed with water then cold aqueous ethanol and dried to give pure bis(3,4-methylenedioxy)chalcone DC-0006B (476 mg, 53%).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08586585B2
Quelldatensatzuspto-grants-2013_11
ORD IDord-a5e51fd745c94bc18dfbca97f47fbb3d
Quellennotizuspto-grants-2013_11