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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2049272Erstellt: 26. Oktober 2026

Ethanone, 2-chloro-1,2-diphenyl- → Thiazole, triphenyl-

https://huagongshe.com/reaction/2049272

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEthanone, 2-chloro-1,2-diphenyl-HCID 95343—
EduktThiobenzamideHCID 683563—
LösungsmittelIsopropanolHCID 3776—
ProduktThiazole, triphenyl-HCID 1712256—

Reaktionsschritte

Thiobenzamide (13.7 g, 0.10 mole) and desyl chloride (23.1 g, 0.10 mole) are heated under reflux in isopropyl alcohol (100 ml) for three hours. When the reaction mixture is cooled, the white solid precipitate formed is filtered off, washed twice with isopropyl alcohol, and dried. The yield of triphenylthiazole, m.p. 84°-85.5° C., is 21.5 g or 69%.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04197306
Quelldatensatzuspto-grants-1980_04
ORD IDord-3912ad2349f94687be5fa180fdf6869a
Quellennotizuspto-grants-1980_04