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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2049311Erstellt: 27. Oktober 2026

Triethyl orthoacetate → 1,1,1-Triethoxybutane

https://huagongshe.com/reaction/2049311

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktTriethyl orthoacetateHCID 66221—
Edukt2-ThenoylacetonitrileHCID 141853—
Edukt5-Methyl-beta-oxo-3-thiophenepropionitrileHCID 20345054—
Produkt1,1,1-TriethoxybutaneHCID 371779—

Reaktionsschritte

The general procedure of Example 11 is repeated but replacing the β-oxo-2-thiophenepropionitrile and triethyl orthoacetate employed in that example with equivalent amounts of 5-methyl-β-oxo-3-thiophenepropionitrile and triethyl orthobutyrate whereby there is obtained the title compound in equally good yield.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04197310
Quelldatensatzuspto-grants-1980_04
ORD IDord-f02fa6a482744ddf92cd3ffb5abf0761
Quellennotizuspto-grants-1980_04