HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Chlorophenylhydroxylamine → alpha-p-bromophenyl-N-p-chlorophenylnitrone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Chlorophenylhydroxylamine | HCID 69983 | — |
| Edukt | 4-Bromobenzaldehyde | HCID 70741 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | alpha-p-bromophenyl-N-p-chlorophenylnitrone | HCID 73998147 | — |
Reaktionsschritte
p-Chlorophenylhydroxylamine (0.05 moles) was dissolved in warm 95% ethanol (20 cc) and was treated with p-bromobenzaldehyde (0.05 moles) with vigorous stirring. The solid which formed was collected, washed with 95% ethanol, and was recrystallized from ethanol to give α-p-bromophenyl-N-p-chlorophenylnitrone.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04197314 |
| Quelldatensatz | uspto-grants-1980_04 |
| ORD ID | ord-9f43e82fb3f0460c8f3e6bf9d55c01f4 |
| Quellennotiz | uspto-grants-1980_04 |