Ethanol → HCID 20344096, Verbindung

HRID 2049628Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2049628
[F:1][C:2]1[CH:3]=[C:4]([CH:15]=[CH:16][CH:17]=1)[O:5][C:6]1[CH:14]=[CH:13][CH:12]=[CH:11][C:7]=1[C:8]([OH:10])=[O:9].OS(O)(=O)=O.[CH2:23](O)[CH3:24]>>[F:1][C:2]1[CH:3]=[C:4]([CH:15]=[CH:16][CH:17]=1)[O:5][C:6]1[CH:14]=[CH:13][CH:12]=[CH:11][C:7]=1[C:8]([O:10][CH2:23][CH3:24])=[O:9]

Komponenten

4

Edukt 3

HCID 702EthanolHCID 1118Sulfuric AcidHCID 203440992-(3-Fluorophenoxy)benzoic acid

Produkt 1

HCID 20344096HCID 20344096, Verbindung

Versuchsvorschrift

2-(3-Fluorophenoxy)benzoic acid (10 g.) and 100 ml of ethanol containing 1 ml. of concentrated H2SO4 were heated at reflux through molecular sieves overnight. The solvent was evaporated, and the residue poured into 50 ml. of 7% NaHCO3. The resulting ester was extracted with ether. ##STR10##

Aufarbeitung

  1. temperatureat reflux through molecular sieves overnight
  2. customThe solvent was evaporated
  3. additionthe residue poured into 50 ml
  4. extractionThe resulting ester was extracted with ether

Quellen und Nachweise

ORD-Eintrag
ord-34832fdf8e0e476fa5110ec0262fc185
Quelldatensatz
uspto-grants-1980_04
Patentnummer
US04198421

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