HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thiocyanic acid, chloromethyl ester → 3-Trifluoromethyl-thiobenzoic acid thiocyanomethyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thiocyanic acid, chloromethyl ester | HCID 76755 | — |
| Edukt | HCID 178526136 | HCID 178526136 | — |
| Produkt | 3-Trifluoromethyl-thiobenzoic acid thiocyanomethyl ester | HCID 54445077 | 69% |
Reaktionsschritte
23 g (0.1 mol) of the K salt of 3-trifluoromethyl thiobenzoic acid and 14.3 g (0.13 mol) of chloromethyl thiocyanate were reacted and processed as in Example 1 B. 19 g of a yellowish oil having a density of 1.4 (this corresponds to a yield of 69% of the theoretical conversion).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04198428 |
| Quelldatensatz | uspto-grants-1980_04 |
| ORD ID | ord-aa3a7781ad23430db1f2ed350d4ff60c |
| Quellennotiz | uspto-grants-1980_04 |