HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Phenethylamine → N-[[3-Methoxy-2-[3-(4-morpholinyl)propoxy]phenyl]methylene]benzeneethanamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Phenethylamine | HCID 1001 | — |
| Edukt | 3-Methoxy-2-[3-(4-morpholinyl)propoxy]benzaldehyde | HCID 2200348 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | N-[[3-Methoxy-2-[3-(4-morpholinyl)propoxy]phenyl]methylene]benzeneethanamine | HCID 20298672 | 85,9% |
Reaktionsschritte
3-Methoxy-2-[3-(4-morpholinyl)propoxy]-benzaldehyde (42.5 g) and 18.5 g of phenethylamine are reacted in 150 ml. of toluene following the procedure described in Example 1B, yielding 50.0 g of the title compound, boiling point 229°-234° C. at 0.2-0.3 mm of Hg.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04199528 |
| Quelldatensatz | uspto-grants-1980_04 |
| ORD ID | ord-f2dc57033d814d2f95bad3f756adf4fa |
| Quellennotiz | uspto-grants-1980_04 |