HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methylamine → 3-(Methylamino)-1lambda6-thiolane-1,1-dione hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methylamine | HCID 6329 | — |
| Edukt | 3-Sulfolene | HCID 6498 | — |
| Edukt | 3-Aminotetrahydrothiopene 1,1-dioxide hydrochloride | HCID 2795201 | — |
| Produkt | 3-(Methylamino)-1lambda6-thiolane-1,1-dione hydrochloride | HCID 2770817 | 82,2% |
Reaktionsschritte
The procedure of Example 1 was repeated substituting 50 percent aqueous monomethylamine (174 ml.) for the ammonium hydroxide of Example 1. Sixty-four and seven-tenths grams of a white crystalline solid was obtained for a yield of 82.2 percent of theory based upon the 2,5-dihydrothiophene 1,1-dioxide. The solid sublimes over 180° C. and metls between 205° and 210° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04181806 |
| Quelldatensatz | uspto-grants-1980_01 |
| ORD ID | ord-5cf5a7b6ad154086ba6d79520986fb09 |
| Quellennotiz | uspto-grants-1980_01 |