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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2052542Erstellt: 26. Oktober 2026

Water → Benzenesulfonamide, n-2-pyridinyl-

https://huagongshe.com/reaction/2052542

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktWaterHCID 962—
Edukt2-AminopyridineHCID 10439—
EduktBenzene sulphochlorideHCID 22564087—
LösungsmittelTetrahydrofuranHCID 8028—
ProduktBenzenesulfonamide, n-2-pyridinyl-HCID 261514—

Reaktionsschritte

A solution of 264 g of benzene sulphochloride was added dropwise at 10° to 25° C. to a solution of 282 g of 2-aminopyridine in 1200 ml of tetrahydrofuran. After two hours continuous stirring without further cooling, the mixture was poured into water. The reaction product was suction filtered and washed first with water and then with methanol.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04186019
Quelldatensatzuspto-grants-1980_01
ORD IDord-3eeb4aaf21c44523984185ff1c34f48c
Quellennotizuspto-grants-1980_01