HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydroxylamine → HCID 178495721, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydroxylamine | HCID 787 | — |
| Edukt | 3-(4-cyanophenoxy)-5-[(1S)-2-methoxy-(1-methylethyl)oxy]-N-(1-methyl-1H-pyrazol-3-yl)benzamide | HCID 11654366 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | HCID 178495721 | HCID 178495721 | — |
Reaktionsschritte
Hydroxylamine (50% w/w solution, 1 mL) was added to absolution of 3-(4-cyanophenoxy)-5-[(1S)-2-methoxy-(1-methylethyl)oxy]-N-(1-methyl-1H-pyrazol-3-yl)benzamide (300 mg, 0.74 mmol) in ethanol (3 mL) and the reaction mixture allowed to stir at RT for 18 hours. The volatiles were removed in vacuo to give the desired compound as a colourless foam (325 mg).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07745475B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-7a6808c0ea414610b8722719b8b97a43 |
| Quellennotiz | uspto-grants-2010_06 |