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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 20557Erstellt: 24. Oktober 2026

Hydroxylamine → HCID 178495721, Verbindung

https://huagongshe.com/de/reaction/20557

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktHydroxylamineHCID 787—
Edukt3-(4-cyanophenoxy)-5-[(1S)-2-methoxy-(1-methylethyl)oxy]-N-(1-methyl-1H-pyrazol-3-yl)benzamideHCID 11654366—
LösungsmittelEthanolHCID 702—
ProduktHCID 178495721HCID 178495721—

Reaktionsschritte

Hydroxylamine (50% w/w solution, 1 mL) was added to absolution of 3-(4-cyanophenoxy)-5-[(1S)-2-methoxy-(1-methylethyl)oxy]-N-(1-methyl-1H-pyrazol-3-yl)benzamide (300 mg, 0.74 mmol) in ethanol (3 mL) and the reaction mixture allowed to stir at RT for 18 hours. The volatiles were removed in vacuo to give the desired compound as a colourless foam (325 mg).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07745475B2
Quelldatensatzuspto-grants-2010_06
ORD IDord-7a6808c0ea414610b8722719b8b97a43
Quellennotizuspto-grants-2010_06