HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2057514Erstellt: 25. Oktober 2026
Sodium Acetate → 3-(2,2-Dichloroethenyl)-2,2-dimethylcyclopropane-1-carbonitrile
https://huagongshe.com/reaction/2057514
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Sodium Acetate | HCID 517045 | — |
| Edukt | 4,6,6,6-Tetrachloro-2-cyano-3,3-dimethylhexanoic acid | HCID 20434843 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | 3-(2,2-Dichloroethenyl)-2,2-dimethylcyclopropane-1-carbonitrile | HCID 12898173 | 97,3% |
Reaktionsschritte
4-Chloro-2-cyano-3,3-dimethyl-6,6,6-trichlorohexanoic acid (3.07 g) and sodium acetate (2.05 g; water-free) were dissolved in dimethyl formamide (8.0 ml). The solution was then stirred at 145° C. for 12 hours. The working-up procedure was the same as indicated in Example III and yielded 1.85 g of Compound A with purity 90%. Yield 86%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US04211720 |
|---|
| Quelldatensatz | uspto-grants-1980_07 |
|---|
| ORD ID | ord-c3b5d3798f6a4b1d8a088b947a91d36d |
|---|
| Quellennotiz | uspto-grants-1980_07 |
|---|
