N1-(5-chloro-2-methoxy-4-nitrophenyl)acetamide → 5-Chloro-2-methoxy-4-nitroaniline
Reaktionsgleichung
C([NH:4][C:5]1[CH:10]=[C:9]([Cl:11])[C:8]([N+:12]([O-:14])=[O:13])=[CH:7][C:6]=1[O:15][CH3:16])(=O)C>[OH-].[K+]>[NH2:4][C:5]1[CH:10]=[C:9]([Cl:11])[C:8]([N+:12]([O-:14])=[O:13])=[CH:7][C:6]=1[O:15][CH3:16]Komponenten
3
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
0.5 mol (99.5 g) of 2-acetamido-4-chloro-5-nitroanisole and 125 ml of a solution of potassium hydroxide (140 g of KOH/100 ml of water) are introduced into a 500 ml flask; the mixture is brought to between 100° and 110° C. for one hour and three quarters; the product is dried without heating and washed with water.
Aufarbeitung
- customthe product is dried
- temperaturewithout heating
- washwashed with water
Quellen und Nachweise
- ORD-Eintrag
- ord-c6dbbc4a161a46cb97be7a9cb9ce295a
- Quelldatensatz
- uspto-grants-1980_07
- Patentnummer
- US04211776
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