Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Sodium Chlorate | HCID 516902 | — |
| Edukt | Echinenone | HCID 5281236 | — |
| Katalysator | Iodine | HCID 807 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | Canthaxanthin | HCID 5281227 | 65,3% |
Reaktionsschritte
100 mg of echinenone are dissolved in 10 ml of chloroform under a nitrogen atmosphere and are oxidized with 100 mg of sodium chlorate in 1 ml of water after having added 2 mg of iodine dissolved in 1 ml of chloroform. After stirring for 24 hours at -20° C., 67 mg of canthaxanthin having an all-trans content of 81% are obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US04212827 |
|---|
| Quelldatensatz | uspto-grants-1980_07 |
|---|
| ORD ID | ord-648c87607f584ecda96f203161e74617 |
|---|
| Quellennotiz | uspto-grants-1980_07 |
|---|
