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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2058007Erstellt: 25. Oktober 2026

4-Chlorophenylhydroxylamine → alpha-p-bromophenyl-N-p-chlorophenylnitrone

https://huagongshe.com/reaction/2058007

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt4-ChlorophenylhydroxylamineHCID 69983—
Edukt4-BromobenzaldehydeHCID 70741—
LösungsmittelEthanolHCID 702—
Produktalpha-p-bromophenyl-N-p-chlorophenylnitroneHCID 73998147—

Reaktionsschritte

p-Chlorophenylhydroxylamine (0.05 moles) was dissolved in warm 95% ethanol (20 cc) and was treated with p-bromobenzaldehyde (0.05 moles) with vigorous stirring. The solid which formed was collected, washed with 95% ethanol, and was recrystallized from ethanol to give α-p-bromophenyl-N-p-chlorophenylnitrone.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04214003
Quelldatensatzuspto-grants-1980_07
ORD IDord-586b2f5314c549d1aba2bb22f79e584a
Quellennotizuspto-grants-1980_07