Imidazole → 1-Cyclooctylmethylimidazole

HRID 2058442

Reaktionsgleichung

Reaktionsgleichung von HRID 2058442
[NH:1]1[CH:5]=[CH:4][N:3]=[CH:2]1.[Na].Br[CH2:8][CH:9]1[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1>C(O)C>[CH:9]1([CH2:8][N:1]2[CH:5]=[CH:4][N:3]=[CH:2]2)[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1

Komponenten

5

Edukt 3

HCID 795ImidazoleHCID 5360545SodiumHCID 18459730(Bromomethyl)cyclooctane

Produkt 1

HCID 205502381-Cyclooctylmethylimidazole

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

Imidazole (2.0 g, 0.03 mol) was added to a solution of sodium (0.7 g, 0.03 mol) in dry ethanol (50 ml). The mixture was stirred and heated to boiling when bromomethylcyclooctane (5.5 g, 0.027 mol) was added dropwise. Following the addition, the reaction mixture was stirred and boiled for 15 h.

Aufarbeitung

  1. temperatureheated
  2. additionwas added dropwise
  3. additionthe addition
  4. stirringthe reaction mixture was stirred

Quellen und Nachweise

ORD-Eintrag
ord-17299225e1134e1b85d1cdd3e88ce6e3
Quelldatensatz
uspto-grants-1982_03
Patentnummer
US04317830

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