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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2061917Erstellt: 26. Oktober 2026

Pentadecalactone → 15-Bromopentadecanoic acid

https://huagongshe.com/reaction/2061917

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPentadecalactoneHCID 235414—
EduktSulfuric acid hydrogen bromideHCID 86639474—
Edukt15-(15-Bromopentadecyloxy)pentadecanoic acidHCID 86639475—
LösungsmittelAcetic AcidHCID 176—
Produkt15-Bromopentadecanoic acidHCID 552296—

Reaktionsschritte

The present reaction can be carried out in the presence of acetic acid and can be performed by using acetic acid as a solvent. As described in the above Non-patent Document 11, when concentrated sulfuric acid-hydrogen bromide acid is used and 15-pentadecanolide is reacted, for example, 15-(15-bromopentadecyloxy)pentadecanoic acid, which is difficult to get separated from the target compound 15-bromopentadecanoic acid, is produced as a byproduct. As a result, it becomes difficult to obtain highly pure 15-bromopentadecanoic acid.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08283482B2
Quelldatensatzuspto-grants-2012_10
ORD IDord-e1718c7d159f4af1a81fa7a5cc8e7d71
Quellennotizuspto-grants-2012_10