HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
p-Methylpropiophenone → N-(2-Methyl-6-phenyl-pyrimidin-4-yl)-N'-[1-p-tolyl-propylidene]-hydrazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | p-Methylpropiophenone | HCID 21429 | — |
| Edukt | 4-Hydrazinyl-2-methyl-6-phenylpyrimidine | HCID 824627 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | N-(2-Methyl-6-phenyl-pyrimidin-4-yl)-N'-[1-p-tolyl-propylidene]-hydrazine | HCID 73320072 | — |
Reaktionsschritte
The title compound was prepared from 4-hydrazino-2-methyl-6-phenylpyrimidine (300 mg, 1.5 mmol) and 1-p-Tolyl-propan-1-one (174 μL, 1.05 mmol) in 3.0 mL of ethanol by a procedure similar to example 1, step 4 yielding 110 mg (22%) of a white solid. HPLC Purity: 96%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08288398B2 |
| Quelldatensatz | uspto-grants-2012_10 |
| ORD ID | ord-a4909e30ae9c4eb38b3b8ef8437c01bc |
| Quellennotiz | uspto-grants-2012_10 |