1-(4-bromo-2-methoxyphenyl)-4-methyl-1H-imidazole → HCID 59324068, Verbindung
Reaktionsgleichung
Br[C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH:12]=[C:11]([CH3:13])[N:10]=[CH:9]2)=[C:4]([O:14][CH3:15])[CH:3]=1.[Cl:16][C:17]1[CH:22]=[C:21]([Cl:23])[CH:20]=[CH:19][C:18]=1[N:24]1[C:28]([CH3:29])=[N:27][C:26]([NH2:30])=[N:25]1>>[Cl:16][C:17]1[CH:22]=[C:21]([Cl:23])[CH:20]=[CH:19][C:18]=1[N:24]1[C:28]([CH3:29])=[N:27][C:26]([NH:30][C:2]2[CH:7]=[CH:6][C:5]([N:8]3[CH:12]=[C:11]([CH3:13])[N:10]=[CH:9]3)=[C:4]([O:14][CH3:15])[CH:3]=2)=[N:25]1Komponenten
3
Versuchsvorschrift
Prepared in analogy to example 1b) starting with 1-(4-bromo-2-methoxy-phenyl)-4-methyl-1H-imidazole (WO2009076352) and 1-(2,4-dichloro-phenyl)-5-methyl-1H-[1,2,4]triazol-3-ylamine (Synthesis 1976, 274). The title compound was obtained as a brownish solid (Yield=13%). MS ISP (m/e): 429.1 (100) [(M+H)+].
Aufarbeitung
- customPrepared in analogy to example 1b)