1-(4-chlorobenzyl)-1H-1,2,4-triazol-3-amine → HCID 46214068, Verbindung
Reaktionsgleichung
Br[C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH:12]=[C:11]([CH3:13])[N:10]=[CH:9]2)=[C:4]([O:14][CH3:15])[CH:3]=1.[Cl:16][C:17]1[CH:29]=[CH:28][C:20]([CH2:21][N:22]2[CH:26]=[N:25][C:24]([NH2:27])=[N:23]2)=[CH:19][CH:18]=1>>[Cl:16][C:17]1[CH:29]=[CH:28][C:20]([CH2:21][N:22]2[CH:26]=[N:25][C:24]([NH:27][C:2]3[CH:7]=[CH:6][C:5]([N:8]4[CH:12]=[C:11]([CH3:13])[N:10]=[CH:9]4)=[C:4]([O:14][CH3:15])[CH:3]=3)=[N:23]2)=[CH:19][CH:18]=1Komponenten
3
Versuchsvorschrift
Prepared in analogy to example 1b) starting with 1-(4-bromo-2-methoxy-phenyl)-4-methyl-1H-imidazole (WO2009076352) and 1-(4-chloro-benzyl)-1H-[1,2,4]triazol-3-ylamine from example 3a). The title compound was obtained as a colorless solid (Yield=42%). MS ISP (m/e): 395.1 (100) [(M+H)+].
Aufarbeitung
- customPrepared in analogy to example 1b)
Quellen und Nachweise
- ORD-Eintrag
- ord-a223da5c8d2a4b798042c85bedb611d8