HCID 22478061, Verbindung → HCID 69618503, Verbindung
Reaktionsgleichung
O1C2C=CC(C3C=C(N)C(N)=CC=3)=CC=2OC1.[CH2:18]1[O:26][C:25]2[C:24]([N:27]3[C:31]4[CH:32]=[CH:33][CH:34]=[CH:35][C:30]=4[N:29]=[C:28]3[C:36]3[C:44]4[C:39](=[CH:40][CH:41]=[CH:42][CH:43]=4)[NH:38][N:37]=3)=[CH:23][CH:22]=[CH:21][C:20]=2[O:19]1>>[CH2:18]1[O:26][C:21]2[CH:22]=[CH:23][C:24]([N:27]3[C:31]4[CH:32]=[CH:33][CH:34]=[CH:35][C:30]=4[N:29]=[C:28]3[C:36]3[C:44]4[C:39](=[CH:40][CH:41]=[CH:42][CH:43]=4)[NH:38][N:37]=3)=[CH:25][C:20]=2[O:19]1Komponenten
3
Versuchsvorschrift
By proceeding in a manner similar to Example 235(i) above but using 4-benzo[1,3]dioxol-5-ylbenzene-1,2-diamine [Reference Example 30(k)] there was prepared 3-(5-(5,6-methylenedioxy)phenyl-1H-benzoimidazol-2-yl)-1H-indazole as a white solid. MS: 355.2 (M+H)+. HPLC (METHOD B1): RT=22.04 minutes.
Quellen und Nachweise
- ORD-Eintrag
- ord-40854b4f74d647fda1cf3c715dc43421
- Quelldatensatz
- uspto-grants-2012_10
- Patentnummer