6-Methyl-5-(methylthiomethyl)picolinonitrile → (6-Methyl-5-(methylthiomethyl)pyridin-2-yl)methanamine

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Reaktionsgleichung

[CH3:1][C:2]1[N:7]=[C:6]([C:8]#[N:9])[CH:5]=[CH:4][C:3]=1[CH2:10][S:11][CH3:12].C(C1C=NC=C(CCC(C)C)C=1)#N>>[CH3:1][C:2]1[N:7]=[C:6]([CH2:8][NH2:9])[CH:5]=[CH:4][C:3]=1[CH2:10][S:11][CH3:12]

Komponenten

Edukt 2

HCID 686697466-Methyl-5-(methylthiomethyl)picolinonitrile

HCID 686702083-Cyano-5-isopentylpyridine

Produkt 1

HCID 59569884(6-Methyl-5-(methylthiomethyl)pyridin-2-yl)methanamine

Versuchsvorschrift

(6-methyl-5-(methylthiomethyl)pyridin-2-yl)methanamine was synthesized from 6-methyl-5-(methylthiomethyl)picolinonitrile following the general procedure as described for the 3-cyano-5-isopentylpyridine.

Quellen und Nachweise

ORD-Eintrag: ord-050ddc026dc9415f85b8c2b2bd1bec34
Quelldatensatz: uspto-grants-2012_10
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US08299267B2

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