HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Pyridine → HCID 21409997, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Pyridine | HCID 1049 | — |
| Edukt | 2,2,3,4,4,4-Hexafluorobutyl 11-bromoundecylate | HCID 21409996 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | HCID 21409997 | HCID 21409997 | — |
Reaktionsschritte
The process of producing the surfactant of claim 1 comprising (a) reacting at reflux 2,2,3,4,4,4-hexafluorobutanol and 11-bromoundecanoic acid in presence of methane sulfonic acid as a catalyst and benzene as a solvent to obtain 2,2,3,4,4,4-hexafluorobutyl 11-bromoundecylate and then (b) reacting at reflux 2,2,3,4,4,4-hexafluorobutyl 11-bromoundecylate with pyridine in presence of methanol as a solvent to obtain 2,2,3,4,4,4-hexafluorobutyl 11-pyridylundecylate bromide.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04049668 |
| Quelldatensatz | uspto-grants-1977_09 |
| ORD ID | ord-8486ada63155495d8c3a4f1b0de6f8e9 |
| Quellennotiz | uspto-grants-1977_09 |