Formaldehyde → alpha-[(Dipropylamino)methyl]-3,4,5-trimethoxybenzeneacetonitrile
Reaktionsgleichung
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH2:13][C:14]#[N:15])[CH:6]=[C:7]([O:11][CH3:12])[C:8]=1[O:9][CH3:10].Cl.[CH2:17]([NH:20][CH2:21][CH2:22][CH3:23])[CH2:18][CH3:19].[CH2:24]=O>>[CH2:17]([N:20]([CH2:24][CH:13]([C:5]1[CH:6]=[C:7]([O:11][CH3:12])[C:8]([O:9][CH3:10])=[C:3]([O:2][CH3:1])[CH:4]=1)[C:14]#[N:15])[CH2:21][CH2:22][CH3:23])[CH2:18][CH3:19]Komponenten
4
Versuchsvorschrift
In a manner similar to Preparation 11 react 3,4,5-trimethoxybenzeneacetonitrile with dipropylamine hydrochloride and paraformaldehyde to obtain the title compound.
Aufarbeitung
- customIn a manner similar to Preparation 11