HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cyclopentanone → 1-(Diethylamino)cyclopentanecarbonitrile
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cyclopentanone | HCID 8452 | — |
| Edukt | Potassium Cyanide | HCID 9032 | — |
| Edukt | Diethylammonium chloride | HCID 10197650 | — |
| Edukt | 1-(Dimethylamino)cyclopentanecarbonitrile | HCID 10773049 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 1-(Diethylamino)cyclopentanecarbonitrile | HCID 24276761 | 62% |
Reaktionsschritte
The title compound (2.06 g, 62%) was prepared from diethylamine hydrochloride (2.14 g, 20 mmol), cyclopentanone (1.68 g, 20 mmol) and potassium cyanide (1.30 g, 20 mmol) in water (10 ml) in a similar manner to that described in D1. 1H NMR (CDCl3) δ: 1.11 (6H, t, J=7 Hz), 1.78-1.88 (6H, m), 2.22 (2H, m), 2.71 (4H, q, J=7 Hz).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07745642B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-10ca5a0bc6414f21970b59dd43514c14 |
| Quellennotiz | uspto-grants-2010_06 |