Ethyl Spiro[2.5]octane-1-carboxylate → 6-tert-butylspiro[2.5]octane-1-carboxylic Acid

HRID 2079472

Reaktionsgleichung

Reaktionsgleichung von HRID 2079472
[C:1]([CH:5]1[CH2:17][CH2:16][C:8]2([CH:10]([C:11]([O:13]CC)=[O:12])[CH2:9]2)[CH2:7][CH2:6]1)([CH3:4])([CH3:3])[CH3:2].C1(C(OCC)=O)C2(CCCCC2)C1>>[C:1]([CH:5]1[CH2:17][CH2:16][C:8]2([CH:10]([C:11]([OH:13])=[O:12])[CH2:9]2)[CH2:7][CH2:6]1)([CH3:4])([CH3:2])[CH3:3]

Komponenten

3

Edukt 2

HCID 11206164Ethyl Spiro[2.5]octane-1-carboxylateHCID 67102465Ethyl 6-tert-butylspiro[2.5]octane-1-carboxylate

Produkt 1

HCID 103530726-tert-butylspiro[2.5]octane-1-carboxylic Acid

Versuchsvorschrift

The title compound was prepared as described in Example 1B substituting the product from Example 24B for the product from Example 1A. MS m/z 228 (M+NH4)+.

Quellen und Nachweise

ORD-Eintrag
ord-fc8e7c460a4e488ea2ca9b3972a9d7fa
Quelldatensatz
uspto-grants-2011_04
Patentnummer
US07932245B2

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